US 7,462,336 B2
Apparatus for preparing a dialkyl carbonate
Jan van de Broek, Bergen op Zoom (Netherlands); Stephan Bouwens, Bergen op Zoom (Netherlands); Maarten Campman, Roosendaal (Netherlands); Daniel Favre, Rensselaer, N.Y. (US); Cornelis Adrianus Maria van Gool, Kapellen (Belgium); Leon Kalle, Almere (Netherlands); and George P. Moloney, Jr., Mechanicville, N.Y. (US)
Assigned to Sabic Innovative Plastics IP B.V., Bergen op Zoom (Netherlands)
Filed on Jun. 27, 2005, as Appl. No. 11/167,649.
Application 11/167649 is a division of application No. 10/250067, filed on Jun. 02, 2003, granted, now 6,977,308.
Claims priority of provisional application 60/401916, filed on Aug. 08, 2002.
Claims priority of provisional application 60/391389, filed on Jun. 25, 2002.
Prior Publication US 2005/0265907 A1, Dec. 01, 2005
Int. Cl. C07C 69/96 (2006.01); B01J 8/04 (2006.01)
U.S. Cl. 422—191  [558/277] 7 Claims
 
1. An apparatus for preparing a dialkyl carbonate, comprising:
means for reacting an alkanol, oxygen, carbon monoxide, and a catalyst to form a mixture comprising a dialkyl carbonate, an alkyl chloroformate, hydrochloric acid, water, carbon dioxide, and carbon monoxide;
means for separating from the mixture a gaseous fraction comprising carbon monoxide and alkyl chloroformate; and
means for removing alkyl chloroformate from the gaseous fraction.